直读光谱仪对氩气的要求
发布时间:2021-06-09
<p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">高纯度的氩气对直读光谱仪来说是不可或缺的,不少厂家为了节省成本会采用自己灌装或者采购的低纯度氩气,虽然也能够使用但对于光谱仪的检测结果还是会有影响的。</span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt; mso-ascii-font-family: Calibri; mso-hansi-font-family: Calibri;"> </span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"> <span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">直读光谱仪对于氩气纯度一般要达到</span>99.999%<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">,这样对仪器分析的稳定性较好,如果氩气纯度不够的话,有部分高合金</span>(<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">如</span>Cr<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">、</span>Ni<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">、</span>W<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">等含量高</span>)<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">样品是没有办法正常激发的。</span></span></p><p style="margin: 0pt; text-align: center; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"> <img title="1623202630590265.png" alt="图片1.png" src="/uploads/image/20210609/1623202630590265.png"/></span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">对于很多客服反映直读光谱仪对于氩气的的消耗非常大,正常情况下,一天</span>50<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">个样品,一瓶氩气</span>(14MPa)<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">至少可以用</span>5<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">天以上,如果光谱仪对于氩气消耗特别的大有可能是有漏气或氩气分压表流量太大。供氩气钢瓶的减压器压力为</span>0.60--0.70MPa,<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">管路漏气则消耗氩气多。</span></span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"> </span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">直读光谱仪供氩气有如下几个流量:最低流量</span>6-10<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">升</span>/<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">小时;常流量</span>40-60<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">升</span>/<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">小时,直读光谱仪后面板的激发电源开关开则此流量一直供气,用于冲洗激发室的透光镜片和维持激发室氩气正压力,防止分析间隔过程及更换样品时激发室进入空气;分析流量</span>200--300<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">升</span>/<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">小时,只是激发样品时供气;阀、快门供气,如果管路不漏气耗气量极小。</span></span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"> </span></p><p style="margin: 0pt; line-height: 1.75em;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: Calibri; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;"><span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">所以,激发电源开关</span>24<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">小时开,一瓶气可用</span>3<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">天左右,如果长时间不分析样品</span>(<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">如间隔</span>2<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">小时</span>)<span style="color: rgb(0, 0, 0); line-height: 150%; font-family: 宋体; font-size: 11pt; mso-spacerun: "yes"; mso-fareast-font-family: 宋体; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0000pt;">可关闭直读光谱仪的激发电源开关,但不要关直读光谱仪的总电源。</span> </span></p><p style="line-height: 1.75em;"><span style="color: rgb(0, 0, 0);"> </span></p>